diffractometer相关论文
A diffractometer with W Kα1 characteristic X-ray as X-ray source was designed in house.This diffractometer can realize ......
Synthesis,Crystal Structure,Specific Heat Capacity,Thermodynamic Properties and Heat of Formation of
N-(benzoyl)-N-(2,4-dinitrophenyl amino) thiourea was synthesized via the reaction of2,4-dinitrophenylhydrazine alter wit......
<正> Ⅰ. INTRODUCTION The 1-vinylsilatrane is a compound with the presence of pentacoordinated silicon. Structural studi......
The phase diagrams of binary systems SmCl_3-CaCl_2 and SmCl_3-LiCl were determined byDTA and X-ray diffraction analysis......
Influence of CeO_2 on the Microstructure and Wear Resistance of M_(80)S_(20) Thermal Spray and Therm
The influence of rare earth oxide CeO_2 on microstructure and wear resistance of M_(80)S_(20) thermal sprayand thermal ......
Six different compositions in Bi_2Sr_2Ca_2Cu_3O_y:Se_x. with x=0.0, 0.05, 0.1, 0.2, 0.3, 0.4 have been prepared by the s......
Synthesis, Characterization, X-ray Crystal Structure and Herbicidal Activity of(E)-2-(2,4-Dichloroph
A new crystal of(E)-2-(2,4-dichlorophenoxy)-1-(5,5-dimethyl-2-oxido-1,3,2-dioxaphosphinan-2-yl)vinyl 2-(2,4-dichlorophen......
Two polymorphic forms (forms I and IV) of antidepressant bupropion hydrobro- mides were prepared and characterized by po......
Three new iron(Ⅲ) phosphonate cage-like complexes with [Fe 4 ], [Fe 9 ] and [Fe 14 ] cores have been synthesized by sol......
An alternative aqueous synthetic route to preparing CdTe quantum dots with tunable photoluminescence
An aqueous synthetic route has been developed for the preparation of mercaptosuccinic acid(MSA)-capped CdTe quantum dots......
A novel nonenzymatic glucose sensor was successfully fabricated based on the Cu2O polyhedrons covered Cu foil.The Cu2O p......
Cuprous oxides with different morphologies were formed on F-doped tin oxide (FTO) covered glass substrates by potentiost......
NdFeCo magnetic powder was prepared by the process of smelting,high-energy ball milling and oxidation heat treating.The ......
Synthesis,Structure and Thermal Stability of a Cadmium Coordination Polymer:[Cd(phen)(4,6-dimethyl-5
One cadmium(Ⅱ)coordination polymer [Cd(phen)(4,6-dimethyl-5-nitro-isophtha-lic acid)]n(1)has been synthesized with 4,6-......
Influence of silicon and carbon elements on formation of 1:13 phase and microstructure in LaFe_(13-y
Microstructure dependent on silicon and formation of 1:13 phase in LaFe13-ySiyC0.2 compounds was investigated. C and Si ......
The title compound 4-(N,N-diphenylamino)styrene-4′-N-methylpyridinium iodine (abbreviated to PASMPI) was synthesized by......
An aminophenol ligand, N,N,N′-tri(2-hydroxy-5-methylbenzyl)-1,2-ethanediamine, was prepared through the Mannich reactio......
Vitamin D3 (VD3) proliposomes (VDP), consisted of hydrogenated phosphatidycholine (HPC) and VD3, were prepared using sup......
We have successfully synthesized Sr 2 CuO3+δ single crystals under high pressure and high temperature for the first tim......
The isothermal section of the phase diagram of the Gd-Sm-Co ternary system at 773K was investigated by X-ray powder diff......
Microstructure and isothermal oxidation of 3Al_2O_3·2SiO_2/SiC coating on high and low density carbo
Carbon-carbon composite (C/C) materials are prone to severe oxidation and volatilization problems. To address these issu......
以 SnCl4为前驱体、以氧气和氢气的混合气体为爆源,通过气相爆轰制备纳米二氧化锡粉末。并通过 XRD 和 TEM 等测量手段对纳米 SnO2......
采用X衍射粉末数据对不同温度下处理的铜基气凝胶的晶体结构进行分析,通过对比实验与模拟的XRD图谱模拟出样品1、2、3的晶体结构,......
Synthesis,Crystal Structure and Photoluminescent Property of a New Ca(Ⅱ) Compound Constructed from 5
A new coordination polymer, namely [Ca(HOABDC)]n(1, H3 OABDC = 5-oxyacetateisophthalic acid), has been synthesized throu......
Synthesis,Structure,and Luminescent Property of a 3-D Zinc Complex {[Zn_8~(II)(4-APha)_8(CH_3COO)_8]
The title complex [ZnⅡ8(4-APha)8(CH3COO)8(CH3CH2OH)2]n(1, 4-APha = 4-aminophenylhydroxamic acid) has been prepared unde......
Synthesis, Structure and Norbornene Polymerization Catalyzed by o-Benzene Diimine Di-nuclear Palladi
The title complex, C20H17N4Pd2Cl3·0.5CH3OH, crystallizes in the triclinic system, space group P1 with a = 9.927(6), b =......
Synthesis and Electrochemical Behavior of Electroactive Bistetrathiafulvalene-attached Thiacalix[4]a
Tetrabromoalkylthiacalix[4]arenes(1a and 1b) reacted with excess bis(tetraethylammonium)-bis(1,3- dithiole-2-thione-4,5-......
2D Naphthalenedisulfonate-cadmiun coordination polymer with2,4,5-tri(4-pyridyl)-imidazole as a co-li
A new 2D coordination polymer,[Cd(tpim)(1,5-nds)]_n(1),was constructed from 1,5-naphthalenedisulfonate(1,5-nds),2,4,5-tr......
One-pot synthesis of novel pyrido[2,3-d]pyrimidines using HAp-encapsulated-γ-Fe_2O_3 supported sulfo
Novel pyrido[2,3-d]pyrimidine derivatives were synthesized through a one-pot three-component approach using HAp-encapsul......
Solvothermal Synthesis,Crystal Structure and Properties of a 3D Organically Amine Templated Lanthani
A new sulfate inorganic framework, {(C2H8N)9[Nd5(SO4)12]·2H2O}n(1) templated by organic amine, has been solvothermally ......
Synthesis,Crystal Structure and MMCT Property of a New Mixed-valence Cyanide-bridged Binuclear Compl
A new mixed-valence cyanide-bridged complex, Br3Fe(μ-NC)RuBr(dppm)2(dppm = bis(diphenylphosphino)methane), was obtained......
One novel organically templated zincophophate(C5N2H14)·[Zn3(OH2)(PO4)2(HPO4)] has been synthesized under hydrothermal c......
Epitaxial growth of SmFeO3/SrRuO3 was achieved on SrTiO3 substrates by the pulsed laser deposition(PLD)method at 973 K u......
Synthesis, Crystal Structure, and Topology Analysis of One Novel Interpenetrated 2D Cobalt Coordinat
One novel cobalt coordination polymer, {[Co(HTCB)(4,4’-btb)]·H2O}n(1, H3TCB= 1,3,5-tris(4-carboxyphenyl)benzene, 4,4’......
Synthesis,Crystal Structure,and Magnetic and Water-induced Reversible Transformation Properties of {
A novel NiⅡ complex {[Ni(IBG)(μ-H2O)(H2O)2]·2H2O}n 1(H2IBG = isophthaloylbisglycine) has been synthesized and charact......
A 3D Ba(Ⅱ) Inorganic-organic Hybrid Framework Based on 1,3,5-Benzenetricarboxylic Acid Ligand: Synth
A three-dimensional(3D) barium complex with 1,3,5-benzenetricarboxylic acid(H3BTC), {[Ba1.5(BTC)(H2O)]·(H2O)}n(1), was ......
Nonlinear optical material of a low-dimensional coordination polymer:Synthesis,structure,NLO and flu
Employing unsymmetrical 2-mercapto-5-methyl-1,3,4-thiadiazole and 2,2′-bipyridine as mixed ligands, a new low-dimension......
A New Terbium(Ⅲ) Coordination Compound with 2-Thiophenecarboxylic Ligand:Synthesis and Crystal Struc
A new coordination compound with formula [Tb(2-TC)3(DMF)]n(1, 2-TC = 2-thiophenecarboxylic ligand and DMF = dimethylform......
Structure, Antibacterial Activity and Theoretical Study of the Forming Mechanism of Compound [(5-Met
A new thiosemicarbazone compound derived from 1-phenyl-3-methyl-4-(2-thenoyl) pyrazolone-5(HPMTP) and thiosemicarbazide ......
Facile synthesis of novel fluorinated thieno[2,3-d]pyrimidine derivatives containing 1,3,4-thiadiazo
A series of novel fluorinated thieno[2,3-d]pyrimidine derivatives incorporating 1,3,4-thiadiazole were synthesized by a ......
The title compound 3,3’-(4-dimethylaminobenzylidene)-bis-(4-hydroxycoumarin) 3 was synthesized by the reaction of 4-hyd......
Synthesis and Crystal Structure Analysis of 2-Amino-4,6-bis(diphenoxyl phosphoramide)-1,3,5-triazine
A disubstituted triazine compound, namely, 2-amino-4,6-bis(diphenoxyl phosphorramide)-1,3,5-triazine, which is an inhere......
The macrocyclic ligand -H2 py N2-O3ane(2) was readily prepared in a diluted condition in THF.The mixture of 2 and Ni(O......
A new type of calcium-based regenerable carbon dioxide(CO2) sorbent, CaO-NiO, was synthesized via the sol-gel method. Th......
Plastic supported platinum modified nickel electrode and its high electrocatalytic activity for sodi
A novel plastic/multi-walled carbon nanotube(MWNTs)-nickel(Ni)-platinum(Pt) electrode(PMNP) is prepared by chemical-redu......
Synthesis and Electrical Properties of Ce_(0.95)Er_(0.05)P_2O_7 as Intermediate-Temperature Solid Ox
The intermediate-temperature ionic conducting sample of Ce0.95Er0.05P2O7 was prepared via solid state reaction. The cond......
Two novel Ag coordination polymers based on tetrazole-yl acylamide,Ag(NTAA)(1,H-NTAA=N-(1H-tetrazol-5-yl)acetamide) and ......
Hydrothermal Synthesis, Crystal Structure and Luminescent Property of a New Cd(Ⅱ) Coordination Polym
A new Cd(ΙΙ) coordination polymer with 2-nitroterephthalic acid(H2npa) and 1,4-bis(2-methyl-imidazol-1-yl) butane(bib)......
This paper presents a study on thickness dependent physical properties of cadmium selenide thin films. The films of thic......
Synthesis, Crystal Structure, and Magnetic Property of One 3D Nickel Coordination Polymer Based on 2
One novel nickel coordination polymer, {[Ni(OTP)(bib)1.5(H2O)]·2H2O}n(1, H2 OTP = 2-hydroxy-5-(3?,5?-terephthalic acid)......
