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The title compound2-p-methyloxyphenyl-3a-(2-phenyl-1,2,3-triazole-4-yl)-3,4- dihydro-1,2,4-oxa-diazolo[4,5-d][1,5] benzothiazepine (C31H25N5O2S, Mr = 531.63) has been syn- thesized and its structure was determined by single-crystal X-ray diffraction. The crystal belongs to triclinic, space group P1 with a = 10.888(2), b = 15.115(3), c = 16.702(3), α = 99.90(3), β = 95.21(3), γ = 100.41(3)o, V = 2642.1(9) nm3, Dc = 1.336 g/cm3, Z = 4, F(000) = 1112, μ = 0.162 mm-1 ,λ(MoKα) = 0.071073 nm, R = 0.0357 and wR = 0.1126 for 10620 observed reflections with I > 2σ(I). X-ray analysis reveals that the molecular backbone consists of a tricyclic system with the central seven- membered ring in a twisted boat-like conformation.
The title compound 2-p-methyloxyphenyl-3a- (2-phenyl-1,2,3,4-oxa-diazolo [4,5-d] [1,5] benzothiazepine (C31H25N5O2S, Mr = 531.63) has been syn- theized and its structure was determined by single-crystal X-ray diffraction. The crystal belongs to triclinic, space group P1 with a = 10.888 (2), b = 15.115 (3), c = 16.702 (3) α, α = 99.90 (3), β = 95.21 (3), γ = 100.41 (3) o, V = 2642.1 (9) nm3, Dc = 1.336 g / cm3 (Z = 4, F (000) = 1112, μ = 0.162 mm-1, λ (MoKα) = 0.071073 nm, R = 0.0357 and wR = 0.1126 for 10620 observed reflections with I> 2σ reveals that the molecular backbone consists of a tricyclic system with the central seven-membered ring in a twisted boat-like conformation.