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Cross double Mannich reaction and tandem cyclization were achieved under iodine catalyzed conditions,yielding a series o......
The rapid generation of molecular in a relatively easy manner has made the cycloaddition reaction a powerful tool in the......
Perhydroindan(bicyclo[4.3.0]nonane) was converted in a flow-type apparatus under a hydrogen pressure of 5 MPa on six dif......
Density functional theory study of the mechanism of the acid-catalyzed decarboxylation of pyrrole-2-
The mechanisms of the acid-catalyzed decarboxylation of pyrrole-2-carboxylic acid and mesitoic acid have been investigat......
The synthesis and molecular structure of a new dinuclear copper(Ⅰ) complex [Cu(dppb)(NO 3)] 2 are reported.The compound......
Asymmetric Synthesis and Crystal Structure of (-)-N-[(3R)-3-Cyclohexyl]-3-phenylpropananoyl]bornane-
The title compound (-)-N-[(3R)-3-cyclohexyl]-3-phenylpropananoyl]bornane-10,2sultam (C 25 H 35 NO 3 S,M r=429.60),a deri......
Hydrothermal Synthesis,Crystal Structure and Thermal Stability of a Binuclear Copper(Ⅱ) Complex with
One novel binuclear copper(Ⅱ) complex [Cu 2 (Hpt) 2 (CO 3) 2 (H 2 O) 2 ]·H 2 O with copper carbonate and 3-(pyridin-2-......
Silacycles play a very important role in modern organic chemistry and materials science.Construction of silacyclic skele......
A single crystal of Li3Ba2Ho3(WO4)8 was obtained from a flux of Li2WO4 under an air atmosphere. The structure of the pur......
Synthesis and Crystal Structure of a B-H Activated Compound Containing a Furan Ring and an ortho-Car
A new compound[CpCo(Se_2C_2B_(10)H_9)CH_2C(O)C_4H_3O]has been synthesized and characterized by elemental analysis,IR spe......
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A novel, convenient and efficient approach to the synthesis of pyrrole and imidazole derivatives via the reaction betwee......
Lanthanide-catalyzed cyclocarbonylation and cyclothiocarbonylation: a facile synthesis of benzannula
La[N(SiMe3)2]3 proves to be an efficient catalyst system for the cyclocarbonylation of 1,2-disubstituted benzenes with i......
Transmetalation of carborane-fused zirconacycles to Cu(Ⅱ) induces the C-C coupling reaction to form four-membered rings......
Synthesis,crystal structures and luminescence properties of europium and terbium picolinamide comple
The novel coordination structures of europium and terbium chloride-picolinamide complexes(EuCl_3.(C_6H_6N_2O)_2.5H_2O,Eu......
Solvothermal Synthesis,Crystal Structure and Properties of a 3D Organically Amine Templated Lanthani
A new sulfate inorganic framework, {(C2H8N)9[Nd5(SO4)12]·2H2O}n(1) templated by organic amine, has been solvothermally ......
One novel organically templated zincophophate(C5N2H14)·[Zn3(OH2)(PO4)2(HPO4)] has been synthesized under hydrothermal c......
Intramolecular N H···X (X=F, Cl, Br, and Ⅰ) hydrogen bonding patterns of aromatic amides in the solid state are summ......
Synthesis of alkyl bis(dimethylamino)methylenecarbamodithioates from 1,1,3,3-tetramethylguanidine,CS
An efficient synthesis of alkyl bis(dimethylamino)methylenecarbamodithioates via a one-pot reaction between 1,1,3,3- tet......
Synthesis and characterization of a new open-framework zinc phosphite (4,4-(C_5H_4N)_2(CH_2)_3)·[Zn_
Employing 4,4-trimethylenedipyridine as a template,a new two-dimensional zinc phosphite (4,4-(C5H4N)2(CH2)3)· [Zn3(HPO3......
Intramolecular N-H···X(X = F,Cl,Br,and I) hydrogen bonding patterns of aromatic amides in the solid state are summari......
Synthesis, Characterization and Crystal Structure of (+)-N-[(3S)-3-(4- fluorophenyl)heptanoyl]bornan
The chiral molecule (+)-N-[(3S)-3-(4-fluorophenyl)heptanoyl]bornane-10,2-sultam (C23H32FNO3S, Mr = 421.56), a fluorine-c......
The compound 2-(1-naphthalenylamino)-4-thiazolidinone was synthesized by the reaction of 1-(naphthalene-1-yl)thiourea wi......
Synthesis and Crystal Structure of 1,7,8,9-Tetrachloro-4-benzyl-10,10-dimethoxy-4-azatricyclo(5,2,1,
The crystal structure of 1,7,8,9-tetrachloro-4-benzyl-10,10-dimethoxy-4-azatricyclo-(5,2,1,02,6)dec-8-ene-3,5-dione (C18......
A novel synthetic approach to(?)-Z-recifeiolide 6, a 12-membered-ring lactone which can be selectively isomerized into(E......
Facile, one-pot synthesis of new phenanthridine derivatives through 1,4-dipolar cycloaddition of phe
A facile, one-pot synthesis of new phenanthridine derivatives by a three-component reaction between phenantridine, dialk......
X2Si=Ge:(X = H, Me, F, Cl, Br, Ph, Ar···) is a new species. Its cycloaddition reaction is a new area for the study of......
Mechanism of Pd-catalyzed selective C–H activation of aliphatic amines via four-membered-ring cyclom
A theoretical study is carried out on Gaunt’s palladium-catalyzed selective C(sp3)–H activation of unprotected aliphat......
Synthesis and Crystal Structure of a Three-dimensional Cobalt Coordination Polymer Assembled by Ozag
A three-dimensional cobalt coordination polymer [Co(IMPAA)2]n(1, HIMPAA =(2E)-3-[4-(1H-imidazol-1-ylmethyl)phenyl]acryli......
Aminosilane bearing bulky substituents on nitrogen: LH2(L=Me2Si(NDipp-)2 , Dipp=2,6-diisopropylphenyl) was reacted with ......
Synthesis and Crystal Structure of N-(2-(1-butyl-3-phenylureido)-1H- indol-3-yl)-N-(4-chlorophenyl)b
The title compound N-(2-(1-butyl-3-phenylureido)-1H-indol-3-yl)-N-(4-chloro- phenyl)- benzamide (C_(32)H_(29)ClN_4O_2, M......
Survey of recent advances of in the field of π-conjugated heterocyclic azomethines as materials with
This account gives an overview of our recent work in the area of conjugated azomethines derived from 2-aminothiophenes.I......
With the support by the National Natural Science Foundation of China,the research team led by Prof.Shi Zhuangzhi(史壮志)......
A manganese-catalyzed bicyclic annulation of imines with α,β-unsaturated esters via C–H activation is described, whic......
New [1+1] and 62-membered [2+2] Schiff base macrocycles containing a 2,6-diamidopyridine subunit have been synthesized b......
Syntheses,Crystal Structures,and Magnetic Properties of Cobalt(Ⅱ) Complexes with 1,1-Cyclohexanediac
Two new Co(Ⅱ) coordination polymers,{[Co_3(Hchda)_2(chda)_2(bpp)_2(H_2O)_2]}_n 1 and {[Co(chda)(bpe)(H_2O)]·3H_2O}_n 2......
Two New Chlorovanadates: Ba_8Cs_5V_8O_(24)Cl_(13) with [V_8O_(24)] Ring and MgCsV_2O_6Cl with [VO_3]
Two new crystals of chlorovanadates,Ba_8Cs_5V_8O_(24)Cl_(13)(1) and MgCsV_2O_6Cl(2),were grown in the molten salt media.......
从纤维堆囊菌菌株So0157-2发酵吸附树脂的提取物中分离得到四个天然埃博霉素衍生物,包括两个14元环埃博霉素L(1)和L1(2),以及两个......
A strategic study towards constructing the nine-membered azonane ring system of palhinine A via an a
A proposed strategy for constructing the nine-membered azonane ring system embedded in the isotwistane framework of palh......
In recent years, visible light photoredox catalysis has emerged as an important research area in synthesis. In this revi......
An intramolecular organocatalytic enantioselective aza-Michael reaction of carbamates, sulfonamides and acetamides to a,......
Recyclable bifunctional aluminum salen catalyst for CO_2 fixation:the efficient formation of five-me
A variety of unique Al(salen) complexes functionalized by imidazolium-based ionic liquid(IL) moieties with the salen lig......
Synthesis,Characterization and Antibacterial Activity of 3-(2-(Heterocyclo-2-ylthio)-ethoxy)benzo[d]
Seven novel 3-(2-(heterocyclo-2-ylthio)ethoxy)benzo[d]isothiazoles(3a~3g) have been synthesized and characterized by ESI......
Synthesis and adsorptivity of acryloylmorpholine resin to various fission product elements in nitric
A novel silica-supported resin with a cyclic monoamide of polymerized 4-acryloylmorpholine(Silica-AM) was synthesized, a......
Synthesis and biological evaluation of 5,6,7-trimethoxy-1-benzylidene-3,4-dihydro-naphthalen-2-one a
A series of new combretastatin-A4 analogs were synthesized,in which a six-membered ring connects the linking bridge and ......
Facile three-component synthesis and insecticidal evaluation of hexahydroimidazo[1,2-a]pyridine deri
A series of new hexahydroimidazo[1,2-α]pyridine derivatives were synthesized via convenient and practical three-compone......
The flotation and surface interaction of rutile with nonyl hydroxamic acid were investigated in this work. The results s......
Boroles are five-membered,unsaturated heterocycles with an antiaromatic 4π-electron BC_4 ring.According to Breslow’s e......
The problem of how the nitrogenase is capable of transforming dinitrogen into ammoniahas indeed become one of the hot s......
The phase of AlPO-21 was hydrothermally synthesized in the reactant system of diethylamine-RB-Al_2O_3-P_2O_5-H_2O-C_2H_5......