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本文以呋喃甲酸甲酯为原料,经羟烷基化反应,醇解反应和O-甲基化反应合成(_-~+)-金锦香酸二甲酯甲醚。同时,还发现了制备2-乙烯基呋喃衍生物的新方法。
In this paper, methyl furancarboxylate was used as the starting material to synthesize (_- ~ +) -methoxydimethyl ether from hydroxy alkylation, alcoholysis and O-methylation. In the meantime, a new method for preparing 2-vinylfuran derivatives has also been found.