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首次应用ＨＳＣＣＣ 获得白果内酯和橙皮甙纯品。白果内酯经ＴＬＣ， ＨＰＬＣ／ＲＩ， ＭＳ （Ｅ１） 和ＩＲ 谱鉴定， 橙皮甙经ＨＰＬＣ／ ＵＶ 和ＴＬＣ 鉴定， 均达到定量用对照品的纯度和含量要求。表明ＨＳＣＣＣ 是制备性分离中草药对照品的一种简捷实用的新手段。
The first application of HSCCC resulted in pure products of ginkgolide and hesperidin. The determination of ginkgolides was carried out by TLC, HPLC/RI, MS (E1) and IR spectroscopies. The determination of hesperidin was confirmed by HPLC/UV and TLC. Both of them reached the purity and content requirements of the quantitation standards. It shows that HSCCC is a simple and practical new method for the preparation of isolated Chinese herbal medicine reference substance.