Synthesis and microstructure analysis of composite Nd:YAG/YAG transparent ceramics

来源 :Chinese Optics Letters | 被引量 : 0次 | 上传用户:zohan_rfs
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Transparent Nd:YAG/YAG composite ceramics are synthesized by solid-state reaction method using highpurity Y2O3,Al2 O 3,and Nd2O3 powders as raw materials.The mixed powder compacts are sintered at 1780°C for 10 h under vacuum and annealed at 1450°C for20 h in air.The Nd:YAG/YAG ceramics exhibit a pore free structure with an average grain size of about 30 μm.The microstructure of the Nd:YAG/YAG composite transparent ceramics is studied and there is no interface between Nd:YAG and YAG ceramics.The Nd ion distribution in one grain is also studied,which shows that there is no segregation of Nd ions as in Nd:YAG crystals. Transparent Nd: YAG / YAG composite ceramics are synthesized by solid-state reaction method using high purity Y2O3, Al2 O3, and Nd2O3 powders as raw materials. The mixed powder compacts are sintered at 1780 ° C for 10 h under vacuum and annealed at 1450 ° C for 20 h in air. The Nd: YAG / YAG ceramics exhibit a pore free structure with an average grain size of about 30 μm. The microstructure of the Nd: YAG / YAG composite transparent ceramics is studied and there is no interface between Nd : YAG and YAG ceramics. The Nd ion distribution in one grain is also studied, which shows that there is no segregation of Nd ions as in Nd: YAG crystals.
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