Chemical profiling of Jinqi Jiangtang tablets by HPLC-ESI-Q-TOF/MS

来源 :Chinese Journal of Natural Medicines | 被引量 : 0次 | 上传用户:hubaonian
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
AIM:To profile the chemical constituents in Jinqi Jiangtang tablets.METHOD:Based on the chromatographic retention behavior,fragmentation patterns of chemical components,and published literatures,a high-performance liquid chromatography coupled with electrospray ionization quadrupole time-of-flight tandem mass spectrometry(HPLC-ESI-Q-TOF/MS) method was established to characterize and identify components in Jinqi Jiangtang tablets.RESULTS:A total of 52 chemical compounds,including eight iridoid glycosides,seven phenolic acids,twelve alkaloids,six flavonoids,and nineteen saponins,were identified in Jinqi Jiangtang tablets.CONCLUSION:The established method could serve as a powerful tool for structural characterization and quality control of this Chinese herbal preparation. AIM: To profile the chemical constituents in Jinqi Jiangtang tablets. METHHOD: Based on the chromatographic retention behavior, fragmentation patterns of chemical components, and published literatures, a high-performance liquid chromatography coupled with electrospray ionization quadrupole time-of-flight tandem mass spectrometry (HPLC-ESI-Q-TOF / MS) was established to characterize and identify components in Jinqi Jiangtang tablets. A total of 52 chemical compounds, including eight iridoid glycosides, seven phenolic acids, twelve alkaloids, six flavonoids, and nineteen The established methods could serve as a powerful tool for structural characterization and quality control of this Chinese herbal preparation.
其他文献
XPS has been applied to study the reduction influence of the passivated Mo2N sample on H2 chemisorption at room temperature. It is found that most of the Mo6+ s
经验人士总是会提醒发烧友:器材不是万能灵药,但对于职业摄影师来说,一些满足基本拍摄需要的器材装备却是必须的,这些装备就像厨师手中的铁锅、炒勺,是他们必备的劳动工具,只
目的探讨微泡激励的超声空化效应对正常犬前列腺组织的损伤作用。方法15只健康成年雄性犬随机分为超声微泡组、单纯超声组和微泡假照组。在开腹情况下,联合经静脉推注微泡0.1
目的 研究酮洛芬异丙酯在离体裸小鼠和猴皮肤中的渗透和代谢 ,阐明皮肤酯酶代谢的主要活性部位。方法 采用外科手术和酶消化方法制备离体皮肤 ,用水平双室扩散池进行体外渗
目的:评价5种清热类中药注射液(TCMI)引起的BALB/c小鼠腘窝淋巴结反应,探讨清热类注射液潜在的致敏性。方法:70只雌性BALB/c小鼠随机分为阳性致敏组(氯化汞),阴性对照组(生理
(括号内数字为刊期@探索与争鸣体育教学思想起论……………………………………………………………………张洪潭(1)论坯动技能………………………………………………………………
就算在霜冻或者雾蒙蒙的日子里,大自然也为我们提供了大量可以创作出好照片的题材。不过,我们需要对光线、光源有更多的敏感,对曝光有更精细的控制。 Even in frost or mist
江泽民总书记在去年中央人口、资源、环境工作座谈会指出:“我们对国土资源的保护与管理必须严而又严.总的原则是:在保护中开发,在开发中保护.资 General Secretary Jiang Z
1999年6月17日,江泽民主席作了加快开发西部地区的重要讲话之后,西部十省(区、市)各行各业的干部和群众都无不为之振奋并正积极准备,力争在西部地区的大开发中作出更大的贡献
研究了在碱性介质中,以邻菲啰啉为活化剂,锰(Ⅱ)催化高碘酸钾氧化苯酚红褪色指示反应及其动力学条件,建立了测定痕量锰的新方法。锰的浓度在0~0.07μg/mL范围内为线性关系,检测限为3.0ng/mL。用于盐酸