Fabrication of micro-fine high Nb-containing TiAl alloyed powders by fluidized bed jet milling

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A fluidized bed jet milling process was used to make micro-fine high Nb-containing TiAl alloyed powders from the chippings obtained by crushing the Ti-45Al-8.5Nb-(W,B,Y) ingot.The influences of classifier frequency on powder characteristics were investigated.The results show that the powders with controlled average particle size can be prepared on a large scale.The powders with different sizes are all dominated by γ with aminor amount of α2-Ti3Al.The particle size significantly decreases with the classifier frequency increasing.At a classifier frequency higher than 38 Hz,the average particle size of the ground powders is lower than 25μm.The powders are composed of two differ-ent sizes of particles:shaped particles and some clastic particles,and both particle sizes meet the log-normal distribution.With the classifier frequency increasing,the both sizes decrease;meanwhile,the proportion of the clastic particles gradually increases,and the size distribution span value of the ground powders increases correspondingly. A fluidized bed jet milling process was used to make micro-fine high Nb-containing TiAl alloyed powders from the chippings obtained by crushing the Ti-45Al-8.5Nb- (W, B, Y) ingot. These influences of classifier frequency on powder characteristics were investigated.The results show that the powders with controlled average particle size can be prepared on a large scale.The powders with different sizes are all dominated by γ with aminor amount of α2-Ti3Al.The particle size significantly decreases with the classifier frequency increasing. At a classifier frequency higher than 38 Hz, the average particle size of the ground powders is lower than 25 μm. The powders are composed of two differ-ent sizes of particles: shaped particles and some clastic particles, and both particle sizes meet the log-normal distribution.With the classifier frequency increasing, the both sizes decrease; meanwhile, the proportion of the clastic particles gradually increases, and the size distribution span value of the ground pow ders increases correspondingly.
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