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Superfine graphite powder was prepared by bali-milling exfoliated graphite containing anhydrous CuCl_2 in planetary ball milling systems.Nano-scale CuCl_2 graphite intercalation compounds were synthesized by heating a mixture of anhydrous CuCl_2 and graphite nanosheets. Scanning electron microscopy,energy-dispersive X-ray spectroscopy and high-resolution transmission electron microscopy were performed to characterize the microstructures of stage-1 nano-scale CuCl_2 graphite intercalation compounds.The structure and components of the domain wall and core in the nano-scale CuCl_2 graphite intercalation compounds are described.The results show that the content of CuCl_2 in the mixture plays a crucial role in the size of the nano-scale CuCl_2 graphite intercalation compound.
Superfine graphite powder was prepared by bali-milling exfoliated graphite containing anhydrous CuCl_2 in planetary ball milling systems. Nano-scale CuCl_2 graphite intercalation compounds were synthesized by heating a mixture of anhydrous CuCl_2 and graphite nanosheets. Scanning electron microscopy, energy-dispersive X-ray spectroscopy and high-resolution transmission electron microscopy were performed to characterize the microstructures of stage-1 nano-scale CuCl 2 graphite intercalation compounds. The structure and components of the domain wall and core in the nano-scale CuCl 2 graphite intercalation compounds are described. show that the content of CuCl_2 in the mixture plays a crucial role in the size of the nano-scale CuCl_2 graphite intercalation compound.