【摘 要】
：
[VO(Phen)2SO4].4H2O.CH3CH2CHOHCH3(Phen=1,10-邻菲啰啉)在室温下通过溶剂法合成得到,此化合物的晶体结构通过X射线衍射,结构分析和红外表征来确定.结果表明这个化合物属于
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[VO(Phen)2SO4].4H2O.CH3CH2CHOHCH3(Phen=1,10-邻菲啰啉)在室温下通过溶剂法合成得到,此化合物的晶体结构通过X射线衍射,结构分析和红外表征来确定.结果表明这个化合物属于单斜晶系,空间群为P21/c.相应的晶胞参数为a=11.842(4)nm,b=20.263(6)nm,c=12.794(4)nm,β=91.335(5),Z=4,R=0.0466(5323),wR2=0.1613(7030).
[VO (Phen) 2SO4] .4H2O.CH3CH2CHOHCH3 (Phen = 1,10-phenanthroline) was synthesized by a solvent method at room temperature. The crystal structure of this compound was confirmed by X-ray diffraction, structural analysis and IR characterization. The results show that this compound belongs to the monoclinic system with space group P21 / c. The corresponding unit cell parameters are a = 11.842 (4) nm, b = 20.263 (6) nm, c = 12.794 (5), Z = 4, R = 0.0466 (5323), wR2 = 0.1613 (7030).
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