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本文将毛细管气相色谱与Nicolet 5sxc富里叶变换红外光谱联机检测应用于含挥发油的中成药的分析研究。对红灵散中的冰片、麝香酮分别进行了定性定量分析。将红灵散的苯提取液作GC/FTIR定性分析,用气相色谱内标校正因子法测定冰片、麝香酮的含量,其中冰片的加样回收率平均值为100.1％,相对标准偏差为2.0％,麝香酮的加样回收率平均值为97.80％,相对标准偏差为3.5％。
In this paper, capillary gas chromatography and Nicolet 5sxc Fourier transform infrared spectroscopy online detection of volatile oil-containing proprietary Chinese medicines analysis. On the red ghost in the borneol, musk ketone were qualitative and quantitative analysis. GC-FTIR was used to characterize the benzene extract of Hongling San. The content of borneol and musk ketone was determined by gas chromatography internal standard calibration factor method. The average recovery of borneol was 100.1% and the relative standard deviation was 2.0% , The average recovery of musk ketone was 97.80% with a relative standard deviation of 3.5%.