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本文使用气-质联用法对太阳神生物健口服液(甘菊型)进行了是否含性激素的鉴定。“生物健”的萃取物经乙酰化衍生后用GC-MS检测,发现有一化合物的质谱既具有雌酮醋酸酯(简写为E_1~-OAc)质谱的一些特征,又具有1,3,5(10),16-四烯-3,17-二羟基雌二醇二醋酸酯[简写为E_1~-(OAc)_2~-]质谱的一些特征;另一化合物的质谱具有雌二醇二醋酸酯[简写为E_2~-(OAc)_2~-]质谱的一些特征。这两个化合物易被误认为是雌酮和雌二醇的乙酰化物。结论是本试验未发现“生物健”含有雌酮和雌二醇。
In this article, the use of gas-mass spectrometry for the identification of sex hormones was carried out on the sun god Bijian oral liquid (camomile type). The “bio-biological” extract was deacetylated and detected by GC-MS. The mass spectrum of a compound was found to have some characteristics of estrone acetate (abbreviated E_1~-OAc) mass spectrometry and 1,3,5 ( 10) Some characteristics of 16-tetraene-3,17-dihydroxyestradiol diacetate [abbreviated as E_1~(OAc)_2~-] mass spectrometry; mass spectrometry of another compound with estradiol diacetate [Abbreviated E_2~-(OAc)_2~-] Mass Spectrometry. These two compounds are easily mistaken for the acetylation of estrone and estradiol. The conclusion is that this experiment did not find “bio-health” containing estrone and estradiol.