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本文用凝胶法合成了晶体配合物［Ｋ（１８－冠－６）］２［Ｃｏ２：Ｉ６］；对其进行了熔点测定、元素分析和红外光谱分析，并做了Ｘ－射线单晶衍射实验．
In this paper, the crystal structure [K (18-crown-6)] 2 [Co2: I6] was synthesized by gel method. The melting point, elemental analysis and IR spectra of the complex were analyzed and X-ray single crystal diffraction experiment.