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In this work,the hydrogen sorption properties of the LiBH4-Mg2NiH4 composite system with the molar ratio 2∶2.5 were thoroughly investigated as a function of the applied temperature and hydrogen pressure.To the best of our knowledge,it has been possible to prove experimentally the mutual destabilization between LiBH4 and Mg2NiH4.A detailed account of the kinetic and thermodynamic features of the dehydrogenation process is reported here.