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以硝基苯为原料在弱酸性条件下 ,利用锌粉还原合成苯基羟胺 ,讨论了反应温度对产物得率的影响 ;在酰卤试剂作用下生成N_酰化苯基羟胺 ,并用FTIR和1H -NMR表征合成产物苯基羟胺及其衍生物
Under the condition of weak acidity, nitrobenzene was used as raw material to synthesize phenylhydroxylamine with zinc powder. The effect of reaction temperature on the yield of product was discussed. The N-acylated phenylhydroxylamine was formed under the action of acyl halide reagent, 1H-NMR Characterization of Synthetic Phenylhydroxylamine and Its Derivatives