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A three-dimensional organic-inorganic hybrid material of [Cd15(OH)4(SO4)4(L1)6(L2)12]n has been prepared via hydrothermal reaction of 3CdSO4·8H2O, 1,2,3-1H-Triazole (HL1) and 5-Methyl-1H-Tetrazole (HL2).The emission spectrum of the title complex in solid state at room temperature shows that the intense emission occurs at 410 nm, which may be assigned to ligand to metal charge-transfer band.