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萤光X光谱分析要求标准样品和分析样品的状态尽可能一致,以消除第三元素的影响,保证分析结果的准确可靠。通常将铌合金标样用金属氧化物合成,由于这种标样和分析试样形态不同,第三元素的影响非常显著。化学处理的方法应用比较广泛,它能使标样和分析试样的形态比较接近,分析精确度大为提高,然而对于我们要分析的NbWAlMoTiZr六元合金,既存在手续繁杂,时间冗长的问题,且因样品中Mo、Al溶解困难、
Fluorescent X-ray spectroscopy requires that the standard and analytical samples be as uniform as possible to eliminate the effects of the third element and ensure accurate and reliable analysis. Usually the niobium alloy standard with metal oxide synthesis, due to the standard sample and analysis of the sample morphology, the third element of the impact is very significant. Chemical treatment method is widely used, it can make the standard sample and analysis of the sample morphology is closer to greatly improve the accuracy of analysis, but we have to analyze the NbWAlMoTiZr six alloy, both complicated procedures and lengthy problems, And due to the sample dissolved in Mo, Al difficult,