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Using 1,1?-bis(isoquinoline)-1,4-phenyldimethylenyl(BIQPM2+) cation as template, a new tetrameric(Bi4 I16)4-iodobismuthate-containing hybrid with formula of(BIQPM)2(Bi4 I16)·H2 O(1), has been prepared under solvothermal conditions. The centrosymmetri