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The hydrothermal reaction of Zn(NO3)2, NaN3, and 1-(4-pyridyl)-2-(2-cyanobenzene) ethylene (PCE), at the mole ratio 1:2:2 in methanol and water at 70 ℃ for two days afforded [Zn(PCE)2(N3)2], the structure of which features a four-coordinated distorted tet