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A Fe-based metal-organic framework,[Fe(INAIP)(DMF)]n·0.5nDMF(1),has been synthesized by the reaction of 5-(isonicotinamido)isophthalic acid(H2INAIP)with FeSO4·7H2O under DMF reaction solvent.Single-crystal X-ray diffraction analysis indicates that complex 1 displays a two-fold interpenetrated three-dimensional(3D)framework with sra topology.The TG,magnetic and adsorption properties of the complex were also studied.