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按1995年版《中国药典》方法测定不同地区高良姜的挥发油含量,以及用环己酮作内标、程序升温毛细管气相色谱法测定挥发油中1,8-桉油素的含量。结果显示:不同地区高良姜的挥发油含量各有差异,在0.84%~1.30%之间,其主要成分1,8-桉油素含量为0.268%~0.501%,占挥发油的29.8%~39.8%。1,8-桉油素在2.709~6.574μg的范围内呈线性关系,γ=0.9999,平均回收率为99.3%(n=4,RSD=2.4%)。方法精密度高,重复性好,操作简便。
According to the 1995 edition of “Chinese Pharmacopoeia” method to determine the volatile oil content of Galangal in different regions, and the use of cyclohexanone as an internal standard, temperature-programmed capillary gas chromatography determination of volatile oil in 1,8 - quercetin content. The results showed that the volatile oil content of Galangal varied in different regions, ranging from 0.84% to 1.30%. The main components of 1,8-aranein content were 0.268% to 0.501%, accounting for 29.8% to 39.8% of volatile oil. 1,8-arbutin showed a linear relationship in the range of 2.709-6.574 μg, γ=0.9999, and the average recovery was 99.3% (n=4, RSD=2.4%). The method has high precision, good repeatability and easy operation.