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首次采用GC及GC/MS方法分别对苄基氯、对硝基苄基溴与多硫化钠反应进行了分析,并确定了反应的中间体结构:节基二硫化物及氨基苄基硫化物。通过对反应过程研究与讨论,为PNT与多硫化钠反应机理研究提供了证据。
For the first time, the reactions of benzyl chloride, p-nitrobenzyl bromide and sodium polysulfide were analyzed by GC and GC / MS respectively. The intermediates of the reaction were identified as: nodisulfide and aminobenzyl sulfide. Through the research and discussion on the reaction process, it provides evidence for the study of the reaction mechanism between PNT and sodium polysulfide.