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A new compound, {[Sm2L3(H2O)4]·(4,4?-bpy)·3H2O}n(1, H2 L = 5-(3-pyridyl methoxy) isophthalic acid, 4,4?-bpy = 4,4?-dipyridyl), has been hydrothermally synthesized and characterized by single-crystal X-ray diffraction. It crystallizes in triclini