【摘 要】
：
The title compound, 1,4-dimethyl-2,5-di{[2’-(3-pyridylmethylaminoformyl)phenoxyl]- methyl}benzene perchlorate (C36H36Cl2N4O12, Mr = 787.59), has been synthesiz
【机 构】
：
State Key Laboratory of Applied Organic Chemistry College of Chemistry and Chemical Engineering Lan
论文部分内容阅读
The title compound, 1,4-dimethyl-2,5-di{[2’-(3-pyridylmethylaminoformyl)phenoxyl]- methyl}benzene perchlorate (C36H36Cl2N4O12, Mr = 787.59), has been synthesized and structurally determined by single-crystal X-ray diffraction. The crystal crystallizes in the orthorhombic system, space group Pbca with a = 14.366(4), b = 15.159(4), c = 16.443(5), V = 3580.9(17)3, Z = 4, Dc = 1.461 g/cm3, μ = 0.253 mm-1, F(000) = 1640, R = 0.0618 and wR = 0.1525 for 1615 observed reflections (I > 2σ(I)). In the structure of the title compound, a two-dimensional supramolecular layer is formed via intermolecular hydrogen bonding interactions.
The title compound, 1,4-dimethyl-2,5-di {[2’- (3-pyridylmethylaminoformyl) phenoxyl] -methyl} benzene perchlorate (C36H36Cl2N4O12, Mr = 787.59), has been synthesized and structurally determined by single-crystal The crystal crystallites in the orthorhombic system, space group Pbca with a = 14.366 (4), b = 15.159 (4), c = 16.443 5, V = 3580.9 173, Z = 4, Dc = 1.461 g / cm3, μ = 0.253 mm-1, F (000) = 1640, R = 0.0618 and wR = 0.1525 for 1615 observed reflections (I> 2σ (I)). , a two-dimensional supramolecular layer is formed via intermolecular hydrogen bonding interactions.
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