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1案例样本及检验1.1简要案情2013年6月某日,在某山坡上发现1具未知名腐败尸体,经法医检验推测,已死亡约8~10d。提取心血,应用LC-MS/MS法检出呋喃丹主要代谢产物呋喃酚[1]。后解剖提取尸体胃内容、肾、心、肝、脑、肺、尿液、心血等,要求进行毒物分析检验。1.2毒物分析检验主要仪器与试剂美国ABI公司API 2000LCMS/MS;岛津公司LC-20A型高效液相色谱仪;呋喃
1 CASE STUDY AND TESTING 1.1 Brief facts On 1 June 2013, an unknown corpse was found on a hillside. According to forensic tests, it has been estimated that it has been deceased for about 8-10 days. Extraction of effort, the application of LC-MS / MS detection of carbofuran major metabolite furanol [1]. Post-anatomical extraction of the contents of the body of the stomach, kidney, heart, liver, brain, lungs, urine, blood, etc., require toxicological test. 1.2 Toxins analysis and testing of major equipment and reagents US ABI company API 2000LCMS / MS; Shimadzu LC-20A-type high performance liquid chromatography; furan