NCDs/TiO2复合材料的制备及其在太阳光下催化制氢的应用

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采用溶剂热法,以乙腈为溶剂和葡萄糖为原料制备了粒径约4 nm的氮掺杂碳量子点NCDs。当激发波长从330 nm增加到470 nm,NCDs水溶液发射光谱出现红移。随后,将一定配比的NCDs、TiO2及5 m L超纯水超声混合60 min,并在80℃烘箱内陈化24 h,NCDs纳米颗粒成功地复合到TiO2(TiO2)表面。该方法有效地拓宽了TiO2吸收光谱的范围,并且减少了光生电子和空穴对,从而增强了TiO2的光催化制氢性能。实验结果表明:投料比为m(NCDs):m(TiO2)=15:85时,以甲醇为牺牲剂
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