【摘 要】
：
6-(Bromomethyl)-4-methoxy-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidin-2-ol(compound 9) was synthesized from 6-methylpyrimidine-2,4-diol(compound 1) through the cru
【机 构】
：
Department of Chemical Biology,State
论文部分内容阅读
6-(Bromomethyl)-4-methoxy-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidin-2-ol(compound 9) was synthesized from 6-methylpyrimidine-2,4-diol(compound 1) through the crucial steps of 6-methyl alkylating and intramolecular cyclization.The assignment of the structure of compound 9 was performed by its spectral data,1H NMR,13C NMR,HMBC,and HRMS spectra.
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