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改进了合成氯乙酸甲酯的方法,并筛选出一种比较合适的溶剂,该溶剂的引入,使连续化反应持续时间更长,使粗品氯乙酸甲酯的含水量大大降低,工艺收率达95%。
The method of synthesizing methyl chloroacetate was improved and a suitable solvent was screened out. With the introduction of the solvent, the duration of the continuous reaction was longer, the water content of the crude methyl chloroacetate was greatly reduced, and the process yield was up to 95%.