【摘 要】
：
建立胃复宁片的质量标准。采用薄层色谱法对胃复宁片中的延胡索和白术进行鉴别;采用HPLC测定胃复宁片中延胡索乙素的含量。薄层色谱斑点清晰,阴性对照无干扰;延胡索乙素含量
【机 构】
：
西安医学院药学院,西安步长医药有限公司,
论文部分内容阅读
建立胃复宁片的质量标准。采用薄层色谱法对胃复宁片中的延胡索和白术进行鉴别;采用HPLC测定胃复宁片中延胡索乙素的含量。薄层色谱斑点清晰,阴性对照无干扰;延胡索乙素含量在0.22—1.10μg范围内与峰面积呈良好线性关系(r=0.9992);平均回收率为97.1%,RSD=2.09%(n=6)。方法简单、准确、重现性好,可有效地控制胃复宁片的质量。
Establish the quality standard of Fufang Ning tablets. The TLC and HPLC were used to identify the Rhizoma Corydalis and Rhizoma Atractylodis Macrocephalae. The content of Tetrahydropalmatine in Ding Fu Ning tablets was determined by HPLC. The results showed that there was a good linear relationship between the content of tetrahydropalmatine and the peak area in the range of 0.22-1.10μg (r = 0.9992), the average recovery was 97.1% and the RSD was 2.09% (n = 6 ). The method is simple, accurate and reproducible, which can effectively control the quality of Fufangning tablets.
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