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The corrosion resistance of NiCrAl +(ZrO2 + Y2 O3 )thermal barrier coating, formed with the plasma spraying technique, on the 18 - 8 steel surface was investigated. The phase structure and morphology of the coating were analyzed by means of X-ray diffraction(XRD) and scanning electron microscopy(SEM). The electrochemical corrosion behavior of the coating in 1.0 mol/L H2 SO4 solution was studied by using electrochemical measurement methods. The results show that the gradient plasma spraying coating is composed of the NiCrAlY primer coating and the (ZrO2 + Y2O3 ) top coating, and the coating thickness is 360 μm. The microhardness of coating reaches 1 100 HV. The corrosion resistance of the plasma sprayed coating of the 18 - 8 steel surface is about 5 times as great as that of the original pattern. The corrosion resistance of the coating is enhanced notably.