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在以往十多年中,XPS技术用于稀土元素氧化物与卤化物,探讨了稀土元素的内壳谱及其伴峰现象,但对稀土元素配合物的研究报导甚少。本文报导我们新合成的稀土元素-吡啶氧正离子硼氢配合物[Ln(PyO)_7]_2(B_(10)H_(10))_3的XPS及其价带谱结果,而这些研究尚未见文献报导。
In the past ten years, XPS technology has been applied to rare earth oxides and halides, and the inner shell spectra and its accompanying peak of rare earth elements have been discussed. However, rare earth element complexes have been reported. This paper reports the XPS and its valence band spectra of the newly synthesized rare earth element-pyridine oxycation ion borohydride complex [Ln (PyO) _7] _2 (B_ (10) H_ (10)) _3 Literature reports.