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A new compound based on polyoxovanadate [{Ni(en)2}2Sb8V14O42]·5.5H2O(en=ethylenediamine)(1) was synthesised hydrothermally as black rhombus crystals.Compound 1 crystallized in the monoclinic system with space group P21/n,Z=4,a=1.46953(9) nm,b=1.28623