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Two new ethoxycarbonylmethyl viologen induced metal halide-based hybrids, (AeV)2(Bi4I16)(DMF)2(1)and (AeV)(CoCl4)(2)(AeV2+=N,N′-bis(ethoxycarbonylmethyl)-4,4′- bipyridinium)have been synthesized and structurally determined by X-ray diffraction method.Unde