【摘 要】
：
The title compound (C19H29NO4) has been synthesized by the reaction of propaldehyde with dimedone and hydroxylamine hydrochloride in glycol under microwave irra
【机 构】
：
Department of Chemistry,Lianyungang Teacher's College
论文部分内容阅读
The title compound (C19H29NO4) has been synthesized by the reaction of propaldehyde with dimedone and hydroxylamine hydrochloride in glycol under microwave irradiation, and its structure was determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21/c with a = 12.533(1), b = 13.184(2), c = 11.883(2)(A), ц = 109.06(1)°, V = 1856.0(5)(A)3, Mr = 335.43, Z = 4, Dc = 1.201 g/cm3, λ = 0.71073 (A), ц(MoKаа = 0.083 mm-1 and F(000) = 728. The structure was refined to R = 0.0488 and Wr = 0.1456 for 2306 observed reflections with I > 2б(I). X-ray analysis reveals that the pyridine ring adopts a boat conformation, while two cyclohexanone rings have envelope conformations.
其他文献
In this study,the effects of pre-carburization of catalyst,hydrogen addition to methane feed and the space velocity of methane on the catalytic performance in m
In this letter, using a Backlund transformation and the new variable separation approach, we find a new general solution of the (N+1)-dimensional Burgers system
In this paper, new basic functions, which are composed of three basic Jacobi elliptic functions, are chosen as components of finite expansion. This finite expan
为探究吕家坨井田地质构造格局,根据钻孔勘探资料,采用分形理论和趋势面分析方法,研究了井田7
By using dressing actions of the Gn-1 1,1,n-1-system, the authors study geometric transformations for flat time-like n-submanifolds with flat, non-degenerate no
A new-style flood discharging dam, which consolidates the flaring gate pier and the stepped spillway for discharging the flood through the dam surface, had been
The present work reports the irradiation induced grafting polymerization onto nano-sized CaCO3 particles, mainly focusing on the effects of pretreatment with si
A water-soluble pectin SB1-1 was isolated and purified from the root of Panax ginseng C. A. Mey. The HPLC analysis indicates that SB1-1 is homogenous. Its molec
Direct difference methods have been used to solve the simultaneous non-linear partial differential equations for melt spinning without recourse to linearisation
The dynamic buckling of an elastic-plastic column subjected to axial impact by a rigid body has been discussed in this paper. The whole traveling process of ela