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LuC9H3O6(H2O)5·4H2O, Mr = 528. 3, monoclinic, C2/c, a = 14. 673(3), b=16.930(4), c= 14. 383(4)(?) , β=118.77(2)°, Z = 8, 7 = 3132(1) (?)3, Dc = 2. 24g/cm3, μ(MoKα) = 67.0cm-1, F(000) = 2064, R = 0. 052 for 4080 observed reflections. The Lutetium ion is eight-coordinated by three oxygen atoms, one from a 1, 3, 5,-benzenetricarboxylate ligands, two from another one, and five aqua ligands,forming a polymeric zigzag chain along the [101] direction. The Lu -O distances fall in the range of 2. 229 -2. 404(?).
389 (4) (?), Β = 0.38, (3), and LuC9H3O6 (H2O) 5 · 4H2O, Mr = 528. 3. monoclinic, C2 / 118.77 (2) °, Z = 8, 7 = 3132 (1) (?) 3, Dc = 2.24g / cm3, μ (MoKα) = 67.0cm-1, F (000) = 2064, R = 052 for 4080 observed reflections. The Lutetium ion is eight-coordinated by three oxygen atoms, one from a 1, 3, 5, -benzenetricarboxylate ligands, two from another one, and five aqua ligands, forming a polymeric zigzag chain along the [101 ] direction. The Lu -O distances fall in the range of 2. 229 -2. 404 (?).