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A novel coordination polymer [(C10H16N)2(Pb2I6)· 2DMF· H2O]n (C10H16N=N-butyl-2-Methy-Pyridinium) was syn thesized by the reaction of Pb(NO3)2 with C6H10NI at room temperature in DMF solvent and structurally character ized by means of X-ray sing