A novel porphyrin-Schiff base was synthesized via the condensation of 5-(4-aminophenyl)-10,15,20-triphenylporphyrin and ethyl vanillin. After analyzing the level of purification of the porphyrin-Schiff base, it was successfully separated. This porphyrin-Schiff base was characterized by using UV-Vis, IR, 1H NMR and MS spectroscopy. A novel porphyrin-Schiff base was synthesized via the condensation of 5- (4-aminophenyl) -10,15,20-triphenylporphyrin and ethyl vanillin. After analyzing the level of purification of the porphyrin-Schiff base, it was successfully separated. porphyrin-Schiff base was characterized by using UV-Vis, IR, 1H NMR and MS spectroscopy.