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本文采用SeSO2-3-KIO3体系示波极谱催化波法测定了鸡蛋中的硒。试样经HNO3-HClO4混酸消化处理,用浓盐酸还原为Se(Ⅳ)后,进行示波导数极谱测定。该方法线性范围为0.05~2.50μg/L,回收率95%,对样品测量的相对标准偏差为4.76%。
In this paper, SeSO2-3-KIO3 system oscillopolarographic catalytic wave method for the determination of selenium in eggs. The sample was digested with HNO3-HClO4 mixed acid and then reduced to Se (Ⅳ) with concentrated hydrochloric acid. The linear range of this method is 0.05 ~ 2.50μg / L, the recovery rate is 95%, and the relative standard deviation of measurement to the sample is 4.76%.