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A novel 2-D {[Cd4(tpt)2(Cl)4(2,4-pdc)2]·4H2O}n(1) has been synthesized from the hydrothermal reaction of 3,5,6-tris(2-pyridyl)-1,3,5-triazine(tpt), hydrated CdCl2, and 2,4-dicarboxylic acid(2,4-H2pdc). Compound 1 crystallizes in triclinic, P1 space g