Synthesis and Crystal Structure of N-(5-Phenylseleno)pentyl Succinimide

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N-(5-phenylseleno)pentyl succinimide 1, C15H19NO2Se (Mr = 324.27), was prepared by treating Br(CH2)5SePh with potassium succinimide. Its crystal structure has been determined by X-ray single-crystal diffraction. The crystal of 1 belongs to monoclinic system, space group P21/c with the crystal cell parameters: a = 18.018(6), b = 5.980(2), c = 14.682(5) ? = 109.977(6)? V = 1486.7(9) 3, Z = 4, Dc = 1.449 g/cm3, (MoK? = 2.523 mm-1, F(000) = 664,the final R = 0.0302 and wR = 0.0666 for 2623 independent observed reflections with I > 2(I). Structure analyses revealed that there exist strong nonclassical hydrogen bonds (CH…O). N- (5-phenylseleno) pentyl succinimide 1, C15H19NO2Se (Mr = 324.27), was prepared by treating Br (CH2) 5SePh with potassium succinimide. Its crystal structure has been determined by X-ray single- belongs to monoclinic system, space group P21 / c with the crystal cell parameters: a = 18.018 (6), b = 5.980 (2), c = 14.682 (5)? ​​= 109.977 (6)? V = 1486.7 , Z = 4, Dc = 1.449 g / cm3, (MoK? = 2.523 mm-1, F (000) = 664, the final R = 0.0302 and wR = 0.0666 for 2623 independent implied with I> 2 (I). Structure analyses revealed that there exists strong nonclassical hydrogen bonds (CH ... O).
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