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In this work, liquid–liquid equilibria(LLE) data for the ternary system methyl tert-butyl ketone(MTBK)+ o, m,p-benzenediol + water were investigated at 333.2 K, 343.2 K and 353.2 K under 101.3 kPa. The performance of MTBK to extract o, m, p-benzenediol fr