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用一定量盐酸中和不同量醋酸钠,以溴酚蓝为指示剂,分光光度法(592,442nm)测定复方制剂中醋酸钠含量。比较了浓度对单波长值(A)、双波长值(Y)直接线性回归及两者的类似logit变换线性拟合回归的效果。结果表明,变换拟合回归效果满意,醋酸钠在处方量±15%范围内有较好的回收率(A_(592)法:99.54%±0.34%;Y法:100.09%±0.405%),尤以单波长法为简单。处方中其它组分对测定影响小。
A certain amount of hydrochloric acid neutralization of different amounts of sodium acetate, bromophenol blue as an indicator, spectrophotometry (592,442 nm) Determination of sodium acetate content in the compound. The effects of concentration on the linear regression of single wavelength (A), dual wavelength (Y) direct linear regression and their similar logit transformation were compared. The results showed that the regression fitting effect was satisfactory, and the recovery rate of sodium acetate was within ± 15% (A 592): 99.54% ± 0.34%. Y method was 100.09% ± 0.405%), especially the single-wavelength method is simple. Other components in the prescription have little effect on the assay.