使用内部质量控制的酶水解、液一液萃取法提取，ＧＣ—ＥＣＤ及ＧＣ—ＭＳ／ＭＳ检测 法对体内组织、体液的三唑仑及α－羟基三唑仑进行检测，能够同时定量检测出其他方法 难于检测的。一羟基三哇仑和三哇仑成份。该法具有方法简便、灵敏度高、重现性好、线 性范围广、回收率高的特点，经办案实践，证实能够满足实际办案工作的需要。 Using internal quality control enzymatic hydrolysis, liquid-liquid extraction, GC-ECD and GC-MS / MS detection of in vivo tissue and body fluids of triazolam and α-hydroxy-triazolam detection can be simultaneously quantitative detection Other methods are difficult to detect. Hydroxy trivalen and trivalenol. The method has the advantages of simple method, high sensitivity, good reproducibility, wide linear range and high recovery rate. The method has been proved to meet the needs of actual handling work.