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Precipitates in an 11% Cr ferritic/martensitic steel containing Nd with tempering and creep conditions were investigated using transmission electron microscope with energy-dispersive X-ray spectroscopy. The precipitates in the steel with a tempering condition were identified to be Cr-rich M23C6 carbide, Nb-rich/V-rich/Ta–Nb-rich MX carbides, Nbrich MX carbonitride, and Fe-rich M5C2 carbide. Nd-rich carbonitride, which is not known to have been reported previously in steels, was also detected in the steel after tempering. Most of the Nb-rich MX precipitates were dissolved, whereas the amount of Ta-rich MX precipitates was increased significantly in the steel after a creep test at 600 °C at an applied stress of180 MPa for 1,100 h. No Fe2 W Laves phase has been detected in the steel after tempering.(Fe, Cr)2W Laves phase with a relatively large size was observed in the steel after the creep test.
Precipitates in an 11% Cr ferritic / martensitic steel containing Nd with tempering and creep conditions were investigated using transmission electron microscope with energy-dispersive X-ray spectroscopy. The precipitates in the steel with a tempering condition were identified to be Cr-rich M23C6 carbide , Nb-rich / V-rich / Ta-Nb-rich MX carbides, Nbrich MX carbonitride, and Fe-rich M5C2 carbide. Nd- rich carbonitride, which is not known to have been reported previously in steels, was also detected in the Most of the Nb-rich MX precipitates were dissolved, and the amount of Ta-rich MX precipitates was increased significantly in the steel after a creep test at 600 ° C at an applied stress of 180 MPa for 1,100 h. No Fe2 W Laves phase has been detected in the steel after tempering. (Fe, Cr) 2W Laves phase with a relatively large size was observed in the steel after the creep test.