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首次利用薄层色谱法(TLC)研究3三个解毒剂的合成条件,确定了它们反应的最佳时间和产物的Rf值,用气相色谱对产物进行了定性的纯度分析.
For the first time, the synthesis conditions of three antidotes were studied by TLC. The optimum reaction time and the Rf value of the three antidotes were determined. The purity of the product was analyzed by gas chromatography.