【摘 要】
：
该文采用L-酒石酸修饰Raney镍和硅藻土负载的Ni催化剂,制得了一种具有手性特征的酒石酸修饰的镍催化剂（TA／Raney-Ni）,考察了Raney-Ni的制备条件、NaBr及其他辅助修饰剂的添加、
论文部分内容阅读
该文采用L-酒石酸修饰Raney镍和硅藻土负载的Ni催化剂,制得了一种具有手性特征的酒石酸修饰的镍催化剂（TA／Raney-Ni）,考察了Raney-Ni的制备条件、NaBr及其他辅助修饰剂的添加、修饰条件（pH,温度,时间等）对催化剂性能的影响.该文研究了酒石酸修饰的镍催化剂对乙酰乙酸乙酯的手性加氢作用,考察了各种反应条件（如：反应温度、催化剂与底物的配比、搅拌方式、反应辅助溶剂及助剂等）对反应的影响.该工作对催化剂进行了初步的表征,采用文献方法测定了催化剂表面的酒石酸的负载量和反应前后负载量的变化.
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