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Metal-organic frameworks (MOFs) have been emerging as very promising functional materials for gas storage, separation, heterogeneous catalysis, sensing, and drug delivery due to their high surface area, porosity, and chemical tunability.Highly dispersed palladium nanoparticles (Pd NPs) encapsulated in metal-organic frameworks (MOFs) MIL-101(Cr), MIL-101(Cr)-NH2, MIL-53(Al)-NH2 have been prepared.