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The cathode material plays an important role in lithium-ion batteries,because it mainly decides the cost and performance of lithium-ion batteries.Monoclinic Li3V2(PO4)3 containing three mobile lithium ions can extract and insert two lithium ions reversibly between 3.0 and 4.5 V based on the V3+/V4+ redox couple with a capacity of 133 mAh?g?1.