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对碳酸铝铵合成的工艺条件进行了研究，研究了反应物的滴定次序、溶液浓度及加入速度、反应温度等因素对反应产物的影响。实验结果表明，Al（3＋）周围有足够的碳酸氢铵是生成碳酸铝铵的关键，必须将硫酸铝铵加入到碳酸氢铵溶液中，并且碳酸氢铵的浓度大于1.0mol／L才有可能生成碳酸铝铵。另外，温度越高，越有利于生成碳酸铝铵，但反应温度不能超过60℃。生成碳酸铝铵后，加热至230℃，则碳酸铝铵分解成Al2O3，升温至1200℃，则生成α－Al2O3。
The conditions for the synthesis of ammonium aluminum carbonate were studied. The effects of reaction conditions, such as the titration order of the reactants, the concentration of the solution, the addition rate and the reaction temperature, on the reaction products were studied. The experimental results show that there is enough ammonium bicarbonate around Al (3+) is the key to produce ammonium aluminum carbonate, ammonium sulfate must be added to ammonium bicarbonate solution, and the concentration of ammonium bicarbonate is greater than 1.0mol / L Ammonium aluminum carbonate is generated. In addition, the higher the temperature, the more conducive to the formation of ammonium carbonate, but the reaction temperature can not exceed 60 ℃. After the formation of ammonium aluminum carbonate, it is heated to 230 ° C, and ammonium aluminum carbonate is decomposed into Al2O3. When the temperature is raised to 1200 ° C, α-Al2O3 is formed.