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In this paper, a high calcium high sulfate ash as the main material, adding fly ash, lime, cement, gypsum and some modifiers to prepare autoclaved aerated concrete.The products complies with the technical requirements of GB/T11968-2006.This paper also studies the influence of the physical methods and water ratio on autoclaved aerated concrete by high calcium high sulfate ash aerated concrete.The best ratio of water and Grinding time were found in practice study.